Instrumentation

Microwave reactor

Biotage Initiator 400 W microwave reactor for chemical synthesis in crimp-sealed glass vials (0.5 to 20 mL) under pressure of up to 25 bar.

UHPSFC/MS

Waters UPC2 supercritical chromatograph equipped with a diode array (200-400 nm) and mass (ESI) detectors.

HPLC

High-pressure binary gradient HPLC system Knauer Azura equipped with a diode array and polarimettric detectors, autosampler and a column oven.

Recycling HPLC

Isocratic HPLC system JAI LaboACE with solvent recycling equipped with UV-Vis and RI detectors, and a set of organic GPC columns.

GC-MS

Gas chromatograph Agilent 8890/5977C with mass detection (EI) equipped with liquid sample autosampler and QuickProbe solid sample loader.

Preparative HPLC

Preparative HPLC/Flash chromatograph Interchim PuriFlash P5.250 equipped with diode array (200-800 nm) and ELSD detectors.

CPL spectrometer

Jasco CPL-300 circularly polarized photoluminescence spectrophotometer equipped with a peltier thermostat. 

Glove box

Vigor inert atmosphere glove box filled with argon equipped with a purifier unit and solvent trap (suitable for "wet" chemistry).